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meerkat last won the day on July 7 2017

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    South Africa

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  1. meerkat

    Cane sugar

    The convention for expressing concentrations in mass per volume terms is to use the mass of the solute (in this case, sugar) and the volume of the solution. The solution is the mixture of the solute (sugar) and the solvent (water or spirit). That is why I stated the concentration as "855 gram per liter of syrup". Note that a concentration given in mass/vol terms must always include a reference temperature because the volume changes with temperature, although of course the mass does not. I have seen data where the concentration is expressed as grams of solute per liter of solvent, but this is rare and would always be specifically stated as such because of the general acceptance of the convention described above. So, to make up a syrup of 400 gram per liter at 20°C you would put 400 grams of sugar in a 1 liter container and then add water until the combined volume reaches 1 liter, all the while carefully maintaining the temperature at 20°C. An easier and more accurate way to get to 400 gram per liter at 20°C would be to use a conversion table (or even better, AlcoDens LQ😉) to determine that this concentration is equivalent to 34.8 mass % and simply weigh out the 749.4 grams (= (400 / 34.8) x 65.2) of water and add it to the 400 grams of sugar. In this way you do not have to worry about the temperature.
  2. meerkat

    Heads and tails when using NGS

    @Roger , I'm sure you were just trying to have a bit of fun but you need to see your comments from the perspective of the person who is asking the question. If a person who has openly labelled themself as a newbie gets a very specific reply from a member with a high reputational ranking, such as yourself, then the OP is going to take that reply seriously and will not see it as the facetious comment it is intended to be. The OP may not have been following the "GNS Cost and Availability" thread and would not necessarily see your reply in that context. Also, for someone in the future reading this thread it will mislead and confuse them. To anybody else who is confused by Roger's and my comments, please read the "GNS Cost and Availability" thread for context.
  3. meerkat

    Cane sugar

    Yes, the solubility of sucrose decreases as the alcohol content increases. At 20°C the saturation solubility of sucrose in pure water is about 65 mass% or 855 gram per liter of syrup. If you are making a 100 proof liqueur the solubility limit of sucrose drops to 28 mass% or 285 gram/liter. In the cold winter temperatures of Canada the solubility will be a bit less. I don't have the experience to say whether crystallization will occur in the neck or base of the bottle, but I suppose either would be unacceptable.
  4. meerkat

    Cane sugar

    Jen, unless you have very high sugar loading or very high proof, there should not be a problem with crystallization. Invert sugar is more soluble than sucrose, so that would help if you are aiming for very sweet products. When making up a 1:1 (or any other ratio, for that matter) sucrose syrup it is important to measure the parts by weight rather than by volume. It is very hard to get consistent quantities of granular sugar when measuring volumetrically because the bulk density will vary from bag to bag and from batch to batch. If you want consistent taste and proofing it helps enormously to have consistent quality syrup.
  5. I have added Column L to your spreadsheet and attached it here. A value that has an equal number of occurrences above and below it is called the median (the midpoint of the frequency distribution in stats-speak). Cell L2 initially contained my guess for the median. I have set the values in Column L to be +1 if the actual net fill value in Column H is more than my guessed value for the median, or to -1 if the actual value is less than the guessed median. The total of all the + and - ones in Column L should be zero if there are an equal number of aboves and belows. Excel's Goal Seek function makes it easy to find the actual median using its internal trial and error functions. The median turns out to be 701.6. It is useful to compare this with the mean (the usual understanding of "average") which I have shown in Cell H27. The fact that the mean (701.7) is so close to the median (701.6) is an indication that your data points are normally distributed (i.e. follow the typical bell curve) and this is a "good thing" (tm). Because the median is 4.6 grams lower than your target fill of 706.2 and the median and mean are so similar, I suspect that if you simply increase the target to 710.8 (=706.2+4.6) then you will get a mean value very close to 706.2 and your overs and unders will be roughly equal. 898089352_ExpressfillFillerAudit - mod by HCW.xlsx
  6. meerkat

    Checking Fill Level (27 CFR 19.356)

    @indyspirits, Yes there is. The icon with the ruler next to the beaker calls up the Volume Correction Calculator (which also converts between mass and volume). The calculation below shows that 750 ml at 60°F becomes 756.4 ml at 80°F. Note that the mass remains 706.1 grams and this is why almost everyone prefers to bottle by mass.
  7. meerkat

    Checking Fill Level (27 CFR 19.356)

    In the TTB document SSD:TM:516 they give an example of correcting fill levels for temperature, but don't seems to state the target temperature! Or maybe I just read it too quickly. But they use Table 7 to get the temperature correction factor so I guess the standard fill temperature must be 60°F. https://www.ttb.gov/ssd/pdf/tm516.pdf
  8. meerkat

    Label Requirements for Europe

    I hope that someone can confirm that this is irrelevant, but I wouldn't want you to be blindsided by something you could have been aware of. In the EU everything is measured at 20°C rather than the 60°F used by the TTB. This means that while 80.00 proof converts to 40.00% ABV at 60°F it would be 40.07% ABV at 20°C. This is because alcohol expands more with temperature than water does. I see from the regulations linked by Paul that you would have a volume tolerance of 10 ml on a 750 ml bottle. The volume of 750 ml of 80.00 proof spirit at 60°F would increase by 2.3 ml at 20°C, so this should not be a problem if you plan for it.
  9. meerkat

    proofing spirits proofed with sugars

    Tony, AlcoDens LQ can do that calculation for you. Please write to me at the support address given in the help file included with AlcoDens LQ and I will gladly walk you through a few calculations. The learning curve is a bit steep, but fortunately quite short and with a bit of help you will master it very quickly.
  10. meerkat

    Adjusting Proof for Temperature

    The "official" correction is TTB Table 1. This indicates that an apparent proof of 92 at 85F is equal to a true proof of 81.1. The correction calculator in AlcoDens indicates a true proof of 81.13 My opinion is that the difference between 85F and 60F is rather large to make this correction accurately and it would be better to allow the batch to cool before you make your final gauging. Although the expansion of alcohol-water mixtures is very well known and can be calculated very accurately, the unknown factor is the exact expansion factor of the glass used for the hydrometer. AlcoDens and the Table 4 values are based on typical high quality hydrometers, but this is the one factor that is not known for certain when you are doing the correction. Fortunately the expansion of the glass has a much smaller effect on the reading than the expansion of the spirit, but the smaller the temperature difference that you are correcting for, the better your accuracy will be.
  11. meerkat

    proofing spirits proofed with sugars

    Proofing products with sugar is a bit more complex because there are more numbers to work out what goes where in the calculator. But once you have done that, all you have to do is crank the software handle and the answers pop out. I have found that a big help is to carefully answer the question "what do I want to calculate?". This might seem trite and obvious but (for any problem) having the question well formulated is always a strong pointer to the solution. If you have any problems moving over to LQ you are welcome to throw them at me and between us we are sure to get the answer.
  12. meerkat

    AlcoDens LQ on Linux

    Thanks to all for the kind words and the good information on running AlcoDens on Mac and Linux - it is useful to have all this information in one place. If I look at the size of our installed userbase and try to estimate what fraction of them would prefer a SAAS app to a desktop application I can't see a web version being viable. I believe that it is possible to get a Windows desktop app to work as a web app on a chromebook using Google's Remote Desktop app but I have not done it myself. https://www.howtogeek.com/173353/how-to-run-windows-software-on-a-chromebook/ Although our license allows multiple machines to run on a single license, it looks like this application would only handle one chromebook at a time.
  13. meerkat

    proofing spirits proofed with sugars

    Georgeous, I am very happy to help you with this calculation and I will answer your latest questions below, but if you have further questions specific to the use of AlcoDens LQ please write to me directly at the support address given in the software. I don't want to annoy the rest of the people here by turning this forum into the AlcoDens support forum. You have two options if the product is on the sweet side. The first is to ignore the sugar and allow it to find its own level while correcting the Proof. In the Options panel in the top right corner, when you select Base Liqueur as the Target Quantity then the second option (i.e. "Set Product Target For" ) becomes active. In the previous example I had set this to "Alcohol + Sugar" and then AlcoDens LQ will ensure that the targets for alcohol and sugar are met. If instead, you set this option to "Alcohol only" then the sugar will be allowed to find its own level. If you do this you will find that you only need to add 14.695 lb of spirit and the total volume will be 51.53 gallons. The sugar level will be 0.485 lb/gallon and it would probably be difficult to distinguish this taste from the 0.5 lb/gallon case. The second option would be to set a new sugar target. In this case you would select the "Alcohol + Sugar" option and for example set the sugar loading target to 0.45 lb/gall in the Product panel. Now you would need to add 30.129 lb of spirit and 16.431 lb of water and the total volume would increase to 55.52 gallons. If you have a lab scale it would probably be a good idea to make up several 1 litre samples with varying sugar levels and do some taste testing. The quantities involved would be so small that you could put the unused samples back into the bulk liqueur when the tasting is complete, without affecting the overall alcohol and sugar levels.
  14. meerkat

    proofing spirits proofed with sugars

    The reason that a density meter (or hydrometer) will not work is that if you start with pure water and add alcohol the density will decrease, but if you add sugar to water the density will increase. The way the sugar "works against" the alcohol is called obscuration. So if you measure a density of (say) 0.95 it could have been caused by first adding alcohol until the density reached 0.90 and then adding sugar until the density rose to 0.95. We would say that the sugar has obscured the effect of the alcohol from 0.90 to 0.95. On the other hand, you could achieve a density of 0.95 by adding no sugar at all and only adding enough alcohol to lower the density from 1.0 to 0.95. In both cases the density is 0.95, but the spirit compositions are very different. What the procedure in video 3 is trying to achieve is to take a known volume of spirit containing alcohol, water and sugar and then distilling it until all the alcohol (but only some of the water and none of the sugar) is distilled over into the receiver. The receiver then contains all the alcohol that was in the original volume and if the volume of distillate is made up (with water) to the same volume as the original sample then we can use the standard tables (or density meter) to determine the alcohol content in Vol/Vol terms - since we have collected the full volume of alcohol that was in the original sample and it is now contained in a volume (of alcohol and water only) equal to the original sample.
  15. meerkat

    proofing spirits proofed with sugars

    Taking each of your questions in turn: 1. what is my current proof; how to know?  The surest way is to measure it using the distillation procedure shown in the third video you were referred to earlier. But you could get close by calculation if you do the sums on a mass % basis. You added 184.68 lb of 135 Pf spirit, 196.57 lb water and 25 lb sugar. The total mass you have is therefore 406.25 lb. 135 Pf spirit contains 59.78 % mass alcohol so there was 110.40 lb of alcohol in 406.25 lb total and the mass% of alcohol is 27.18%. The sugar is 25 lb in 406.25 or 6.15 % by mass. AlcoDens LQ will convert this to Proof. So we know that you have overshot the target of 70. 2. How to proof up after the fact back to 70 True proof Assuming you have some more of the 135 Proof available and some sugar, we can regard what you have as the "Base Liqueur" and calculate what you need to add to get to 70 Proof. I have taken the sugar target as 0.5 lb/gallon. If you add 15.19 lb of 135 Pf spirit and 0.85 lb sugar you will finish up with 51.66 gallons at 70 Proof. 3. How to measure this to report to TTB? Once again - Video No 3 is your answer.