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Going continuous? Contemplation of modification to distillation column


SilverSwede

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There is a potential foam issue that I have solved very simply.

I constructed an automatic dosing system, sounds complicated but it is very simple.

Pure soap is a good antifoam agent,

I suspend a block of soap in a wire basket at the highest point the foam is allowed, if the foam touches the soap it dissolves a small amount then the foam bubbled break and it drops away immediately.

If no foam then only a very small amount of soap dissolves by steam contact

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Soap is made by my neighbor from olive oil and lye (caustic soda) no perfumes.

Until a couple of weeks ago it was a stripper only.

I am now adding a second column with plates so it should continuously do the cuts. I am altering the heat recovery system so most of the pre-heat is from bottoms.

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So you're running the soap at the top of the stripper/analyzer? 

 

The soap is a clever idea, sadly dont think it'll work for what I'm building... I was going to try to have a small rectification section at the top of mine which would mean the reflux would be running down over the soap.

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