Jump to content

Beginner problems with New reflux Column


CuHeadRoad

Recommended Posts

First time post on here, be gentle if I'm being a Dingus. So I'm not new to distilling but I've always used a pot still and fire heat. I recently built a electrically heated reflux still and I'm having problem. I'll list out the details of my set up then my issues and process.

- 15gal Keg Pot

-single 5Kw heating element. 230v

- 2" reflux column roughly 4ft tall.

- feed and return lines for condenser feed horizontally through the main column to produce the reflux cooling

- cooling water comes in from the bottom and out the top - no packing (yet)

- analog Temp gauge in the boiler - Calibrated RTD at the very top of the column.

- Running 10-12gal of 8-9% sugar wash.

So the problem is that I cannot get any decent proof out of the dang thing. I mean 100proof or less! I see guys on here complaining when they can't get more than 180, so I should by no means be getting the junk output i'm getting. After I get my forshots to run off, I cannot get any output worth a damn until the top of my column hits almost 205F!!! I had it sitting at 170-180F for over an hour and couldn't get more than a few drips. tried 190s barely anything, only after it's over 200 will I start to get steady drip, drip drips. At this point my analog gauge in the boiler is reading 200-210ish. I would have thought that my RTD was out of wack. but the fact that my proof is coming out at 60-100 proof tells me that it's reading correct and that I'm just pulling a ton of water with my ethanol because my temp is too high.

As I mentioned above I'm testing this out with about 10-12gallons of a 8-9% sugar wash that I tested with a hydrometer (I'm not guessing) I would expect to pull at least a gallon of higher proof stuff out. Hell i'm honestly happy with 130-150, let alone what I read these other guys pull out of their reflux stills. I've done 3 runs now and each time I give up after pulling off a quart because after a quart of 70-100proof it drops way down to the floor at like 30 proof :( I've played around with turning my power and water ratios up and down all other the spectrum and I can't get any better results. Any ideas are greatly appreciated. i'm pulling my hair out.

Link to comment
Share on other sites

OK so something is wrong as you can to 160 proof with just a simple pot still on a spirit run.

Do you have a deflegmator at the top of the column?  What type of still is it? CM, VM, CCVM. LM, plates (how many), etc?

Without packing you basically have a tall pot riser with/without a deflegmator so you aren't doing yourself any favor without packing.

Can you post a pic of your setup?

Something is definitely wrong with your setup/running of the still as even on a pot still 50%/100 proof is tails territory on a spirit run.

Are you an experienced distiller to start with?  I ask this to confirm you know you have a good ferment.  What is the ABV of the ferment and how do you know what the ABV is?  Did you do a strip run first?  What was the ABV of the spirit in the boiler at the time of the run?

Those are just some basic questions to start with.

Link to comment
Share on other sites

I have a similar setup on my trial still, 15 gallon keg, single 5500 watt element, 3" column. and I can run in reflux mode to get 195 or pot mode to get whatever output I desire. What type of heating controller do you run? Are your cooling lines separated or run in one continuous loop?

Link to comment
Share on other sites

I had the same problem. I gave a buddy one of my old reflux stills that I could get 160 proof easily.

All he could get was 70 proof.  he had a propane burner that was putting out too much heat at the lowest setting  and  the temp shot past the sweet spot and was picking up water..  We put in a smaller burner that could hold the temp 170 -190 F AND WE GOT it making 170 p   

Link to comment
Share on other sites

Create an account or sign in to comment

You need to be a member in order to leave a comment

Create an account

Sign up for a new account in our community. It's easy!

Register a new account

Sign in

Already have an account? Sign in here.

Sign In Now
×
×
  • Create New...